Active Noise Control (ANC) system emphasizes at USAge of adaptation algorithm and adaptive control structure. In this research is presented experimental result of active noise control system at free space using Diagonal Recurrent Artificial Neural Network control structure. The objective of this research is to develop an Extended Kalman Filter (EKF) algorithm for Diagonal Recurrent Artificial Neural Network control structure, named as Extended Kalman Filter Diagonal Recurrent (EKFDR) algorithm. Experimental result shows that amount of neuron in artificial neural network can be reduced by using diagonal recurrent artificial neural network, without lessening control system performance. Nonlinearity of secondary path in active noise control system can complicate control process. Experimental result shows that diagonal recurrent artificial neural network with EKFDR algorithm produced a better performance than linear controller in compensating of secondary path nonlinearity.